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LIU Hai-xin, ZHANG Nong, WEI Shao-hong. Optimizing post-column derivatize reaction conditions for detecting sulfonamides by high performance liquid chromatograph[J]. Journal of Fisheries Research, 2011, 33(2): 39-43.
Citation: LIU Hai-xin, ZHANG Nong, WEI Shao-hong. Optimizing post-column derivatize reaction conditions for detecting sulfonamides by high performance liquid chromatograph[J]. Journal of Fisheries Research, 2011, 33(2): 39-43.
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Optimizing post-column derivatize reaction conditions for detecting sulfonamides by high performance liquid chromatograph

  • Fujian Fisheries Research Institute,Xiamen 361012,China

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  • Publication Date: June 24, 2011
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    • Abstract
  • Detecting sulfonamindes by post-column HPLC，the effect of sulfonamides derivatized in post-column unite will deeply affect result. Optimizing the main factors which affect the derivatize reaction by orthogonal experiment. The optimal conditions are: mobile phase pH3.0, reaction temperature 60℃, acetonitrile content of mobile phase 18%, concentration of derivatization solution 0.25mg/mL。
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    • References (5)
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